ESRF hc6528 · 400_4 in-situ powder diffraction at ESRF ID22, 900 → 1300 °C · the files, the extraction, the figures · thermomat, Fisika Saila, EHU

Overview

One hundred and one diffraction patterns from 900 to 1300 °C, kept as they came and made legible.

The measurements Irene Urcelay-Olabarria proposed and took with Iñigo González de Arrieta and Mireia Sainz-Menchón at ESRF beamline ID22 (proposal HC-6528, sample 400_4), treated here by Josu M. Igartua so that the team can interpret them: a heating ramp in 25 °C steps, then time series at 1240–1300 °C with a scan every 4.4 minutes, 2.8 hours of them at 1270 °C, and an empty-capillary background; 10.6 hours of beamtime on 10–11 June 2026. The files arrived as bare three-column tables with every piece of metadata in their names. This site records how they were read, what was recovered from them, how the copies were named, and what the numbers and the figures already show (broad maxima from 1000 °C, sharp reflections growing from the 1270 °C hold). The originals are untouched; every copy is checksummed against them on every build.

101
scans from ESRF ID22, 900 → 1300 °C and a background, each copied and checksummed
30
figures through diff-ref-struct (core + drs-publish) · 14 protocol steps
9
findings from the files
15
stages of the experiment, 900 → 1300 °C, 10.6 h of beamtime
Site last built 2026-10-23 22:22