ESRF hc6528 · 400_4 in-situ powder diffraction at ESRF ID22, 900 → 1300 °C · the files, the extraction, the figures · thermomat, Fisika Saila, EHU

Downloads

The data, to download

The 101 scans of the series as received from ESRF ID22, under the names that say what they are, for the members of the team: all of them in one zip, each on its own, the index that maps every file to its original name and carries its checksum, and the plot sets that reproduce the figures in diff-ref-struct. Once the app's interactive map exists, anyone who installs it can open these files and explore the series.

All the scans
hc6528_400_4_renamed.zip · 34.1 MB · 101 files, 112 MB unpacked · SHA-256 fa8afef0464d6a661f3155a37a366bc4ae9151c3267afb6b49b722c1c045a076
The index
file_index.csv: original name → new name, nominal temperature, elapsed seconds, clock start, points, exposure class, SHA-256 of every file
The summary
README.md: layout, format, naming scheme, stages, what the data show, caveats
For the app
hc6528_400_4_drs-sets.zip · 21 kB · the 14 plot and publication sets of the figures, with a README on how to open them in diff-ref-struct
Integrity
Every file's SHA-256 is in the index and in the table below; the zip's is above. The files are the beamline's reduced output as received, byte for byte (the Protocol says what was and was not changed).
Use
Unpublished measurements of the team (Irene Urcelay-Olabarria, Iñigo González de Arrieta, Mireia Sainz-Menchón; data treatment Josu M. Igartua). For the team's work; not to be passed on or published without them.

Each file on its own

The 101 scans under their new names (the original names are in the index). Right-click to save; the browser may show a text file instead of downloading it.

# File Nominal T Elapsed s Class MB SHA-256
001 hc6528_400_4_Qu_001_T0900C_t00000s_long.xye 900 °C 0 long 1.16 da23a0437699318f73a034015bc5cb563286ca559f7dfa2246f584d5899676b2
002 hc6528_400_4_Qu_002_T0925C_t00810s_long.xye 925 °C 810 long 1.16 8104403052637da2c72865ddc150606ca297752adfced80dcd614d6c6bd900af
003 hc6528_400_4_Qu_003_T0950C_t01622s_long.xye 950 °C 1622 long 1.16 e2275ba0ec5f8cb72efd67d7d5371ead931453689aa3f82956662e338c727e31
004 hc6528_400_4_Qu_004_T0975C_t02432s_long.xye 975 °C 2432 long 1.16 580a62701ac7104c0c12681891da78f8867dd07cb95084ac214ad2e21d705008
005 hc6528_400_4_Qu_005_T1000C_t03242s_long.xye 1000 °C 3242 long 1.16 eb53a764b11718451e75a955a3ec39ad968bb321543dcd51d98251f15455a26a
006 hc6528_400_4_Qu_006_T1025C_t04050s_long.xye 1025 °C 4050 long 1.16 a751f251cca6072b0088f768ad473a9be442b0a9c6f68345f48df1cef080b9d3
007 hc6528_400_4_Qu_007_T1050C_t04862s_long.xye 1050 °C 4862 long 1.16 0924ba0692dec38416d0ac0b24afd2aba632cf33eb2e61fc9770f1298e9bf035
008 hc6528_400_4_Qu_008_T1075C_t05672s_long.xye 1075 °C 5672 long 1.16 feb55495ac90a8cf478e4a1a977af20fd8d4ba2cd50d83d79e5813c833cb6b73
009 hc6528_400_4_Qu_009_T1100C_t06482s_long.xye 1100 °C 6482 long 1.16 d005616e2b4d5587714cdbdedb4c92920f6d7e7b23667649fef81386856edf1d
010 hc6528_400_4_Qu_010_T1125C_t07296s_long.xye 1125 °C 7296 long 1.16 783a52a3e9ff5a019aec53f7a9aadcbdaf54e20672b195aa8c8e006d442e9fb4
011 hc6528_400_4_Qu_011_T1150C_t08102s_long.xye 1150 °C 8102 long 1.16 53b90a3b2f3520e8c1edeeeec08f39bbcef36ae364f2946efae7088cc2a62dd2
012 hc6528_400_4_Qu_012_T1175C_t08910s_long.xye 1175 °C 8910 long 1.16 12d2aab01b7ece99f84e3b21905834e18e37df3b00f6630a29769dee0b7c4183
013 hc6528_400_4_Qu_013_T1200C_t09720s_long.xye 1200 °C 9720 long 1.16 fb5909765da1815fb118373ed049aa4058ebba81aee46d2a722b1e8acddc6e86
014 hc6528_400_4_Qu_014_T1225C_t10528s_long.xye 1225 °C 10528 long 1.16 8c061d83070c787b5f99559c52a39bd363c2b8eff978329805aeaed480d34167
015 hc6528_400_4_Qu_015_T1225C_t11156s_long.xye 1225 °C 11156 long 1.16 50f732140f388cafec47b228576a50a967ad182e979a6d0a960fbb3a89bebf29
016 hc6528_400_4_Qu_016_T1240C_t11778s_long.xye 1240 °C 11778 long 1.16 6a44a77f08f9147a6e55c942fe183b81a0f52cc828a0b9e92025e97c30cc2a8d
017 hc6528_400_4_Qu_017_T1240C_t12422s_long.xye 1240 °C 12422 long 1.16 882eae80a6c859bf163410a649712e715373953bcdad143fb06d7cf5f947a1e8
018 hc6528_400_4_Qu_018_T1240C_t12672s_short.xye 1240 °C 12672 short 1.16 4c4427718ee2d3637ab40f39921a85931f07dc69c73dbf7f19ff84cc54df6f83
019 hc6528_400_4_Qu_019_T1240C_t12934s_short.xye 1240 °C 12934 short 1.16 73609aa5282b70dfc84c45a6724cd0a0690757714c52ab19e21bd59e2248aa61
020 hc6528_400_4_Qu_020_T1240C_t13196s_short.xye 1240 °C 13196 short 1.16 3765086d790f24a4eb9cb4196931d1ff85b4ef11b4285a48fd320def9e94e677
021 hc6528_400_4_Qu_021_T1240C_t13458s_short.xye 1240 °C 13458 short 1.16 a39e6dc7b41ea22b4fa899482fb2ff721ee28db70cef844d7c378964dc7a6b94
022 hc6528_400_4_Qu_022_T1240C_t13732s_short.xye 1240 °C 13732 short 1.16 141dc52a31165850491688a4b91ac94572dfa43ff224d5e5fbef4f4c00729e88
023 hc6528_400_4_Qu_023_T1245C_t13992s_short.xye 1245 °C 13992 short 1.16 2abbc87386fe3c69543b96fb2a9af0498fe2c0d2ac28abb28ab39faeb0a112b4
024 hc6528_400_4_Qu_024_T1245C_t14252s_short.xye 1245 °C 14252 short 1.16 3ceb5c510a0834e2c279914429d5256e167e5a78cdc207e6870d6d13eb7271cf
025 hc6528_400_4_Qu_025_T1245C_t14524s_short.xye 1245 °C 14524 short 1.16 e6c12fdfbfb9a7a5a0ac548404393e784b9bf9b6cfb818e5d4c66c6baf8a1e30
026 hc6528_400_4_Qu_026_T1250C_t14786s_short.xye 1250 °C 14786 short 1.16 c2c5db987b9ba630ab2258750e17646b58c2966de5805d2baac9645eb45af40e
027 hc6528_400_4_Qu_027_T1250C_t15046s_short.xye 1250 °C 15046 short 1.16 b737b15a01125cedffc2c136b17194cee0168348c0b865eb7ac6b121fee20480
028 hc6528_400_4_Qu_028_T1250C_t15310s_short.xye 1250 °C 15310 short 1.16 375a4a91cfc886e9897dae4f94c842059b5e1e173b768328ebce9cc4ab9f05ed
029 hc6528_400_4_Qu_029_T1250C_t15570s_short.xye 1250 °C 15570 short 1.16 d5e08cda27b2f704eec6da8d097a4e8cdf91e2dc1f1a1771a3b3809a0eabe528
030 hc6528_400_4_Qu_030_T1250C_t15832s_short.xye 1250 °C 15832 short 1.16 8d69a60bae015cf0c9aa45664595c064186de9004c6b785efeb337c1ec1e5e47
031 hc6528_400_4_Qu_031_T1266C_t16268s_short.xye 1266 °C 16268 short 1.16 a7d693dea340a2d6529e0b0c882db600147a4aab249f7cd05e93d2adf04f34d3
032 hc6528_400_4_Qu_032_T1270C_t16530s_short.xye 1270 °C 16530 short 1.16 0ad753a961da30e1ff5208a092b45138eaa8ac4c229c81f805aa48e029cb4c8b
033 hc6528_400_4_Qu_033_T1270C_t16792s_short.xye 1270 °C 16792 short 1.16 016ed438ff7ec87e45c07bc635e0298bdb6c54209a37f42d54b6e2589b79c474
034 hc6528_400_4_Qu_034_T1270C_t17054s_short.xye 1270 °C 17054 short 1.16 d2affed80f31ccbc75f0592673542a9349521f123f2a6ff5d88b2871fe2f2651
035 hc6528_400_4_Qu_035_T1270C_t17314s_short.xye 1270 °C 17314 short 1.16 048ff83d2634162323ba6e4c167b21cc0744ce7b0848248866f89ace910126d4
036 hc6528_400_4_Qu_036_T1270C_t17578s_short.xye 1270 °C 17578 short 1.16 c035958024a1ff52846a7c31485a0fb3efb77d5e0cba9360f799ef120a800ea5
037 hc6528_400_4_Qu_037_T1270C_t17838s_short.xye 1270 °C 17838 short 1.16 928c7b75b1bbf87a6de67ac9d0b21ea93bb7cf78a81f827704a5aa2a819e34bd
038 hc6528_400_4_Qu_038_T1270C_t18100s_short.xye 1270 °C 18100 short 1.16 8ae042ebba8dfc53cd90f34aed5f659c5b8636f8d73b3b3a2d9f49c203e1d723
039 hc6528_400_4_Qu_039_T1270C_t18362s_short.xye 1270 °C 18362 short 1.16 8a446cf2a76ec254a069cb1932fd3b15b84b508eae177fef01dbc6be9efdf8f8
040 hc6528_400_4_Qu_040_T1270C_t18624s_short.xye 1270 °C 18624 short 1.16 b40e84fe1bdb7f219bce60fa64252928d8dcfeeaf4cefa811d9b1456928028a0
041 hc6528_400_4_Qu_041_T1270C_t18884s_short.xye 1270 °C 18884 short 1.16 67e8fe9b8dc1b985eaec46520fec6dfcd08dd32f805b6a72af746a39bbd517ef
042 hc6528_400_4_Qu_042_T1270C_t19146s_short.xye 1270 °C 19146 short 1.16 1692dfe92bceb0ceec955b986f92a636685cac4125146a5082a9aea419b91897
043 hc6528_400_4_Qu_043_T1270C_t19408s_short.xye 1270 °C 19408 short 1.16 0c6675414bd0418dccfb447de024a620c7816c84edd47fb7ad4a8a94a48ee77f
044 hc6528_400_4_Qu_044_T1270C_t19686s_short.xye 1270 °C 19686 short 1.16 54e755ca7905e6d404a88ac321207d2ed9ed41ae61172abc4e14eb0eb7a25e24
045 hc6528_400_4_Qu_045_T1270C_t19948s_short.xye 1270 °C 19948 short 1.16 61bf1f94920a99b79dcbac2878ce3a88ba9ca6d00ed5018947d69b3f7eff54f9
046 hc6528_400_4_Qu_046_T1270C_t20210s_short.xye 1270 °C 20210 short 1.16 1a26894e77760d6287a59260030d01c2602ea9d3a07fd44c7c46e008c66182ae
047 hc6528_400_4_Qu_047_T1270C_t20472s_short.xye 1270 °C 20472 short 1.16 d03ee44260c8ca1c2ab3477e0628e0c91fa20b929f9c6c763594fefcc0f9d571
048 hc6528_400_4_Qu_048_T1270C_t20734s_short.xye 1270 °C 20734 short 1.16 07443858b9ec33d9382f850d2d0ce6722a5dee137ac94023fc41dda679aadbee
049 hc6528_400_4_Qu_049_T1270C_t20996s_short.xye 1270 °C 20996 short 1.16 8bf2d06fbe0c0c780796af06b17f3695616d70412f1a9f10b3d516b0cbbfe598
050 hc6528_400_4_Qu_050_T1270C_t21256s_short.xye 1270 °C 21256 short 1.16 89b277c677962c90cc14e0f79e62ee684e79df39e9538ac4b80604a9fe614a64
051 hc6528_400_4_Qu_051_T1270C_t21518s_short.xye 1270 °C 21518 short 1.16 84500f12621cf0eab0ece3287a67207d3f15897d70f0de2eb574e90d8b3a767e
052 hc6528_400_4_Qu_052_T1270C_t21778s_short.xye 1270 °C 21778 short 1.16 cb741fd8553bcdf39da7cc633c125d0f8d1535bb4f668b742a32f0ad6f71b3c0
053 hc6528_400_4_Qu_053_T1270C_t22040s_short.xye 1270 °C 22040 short 1.16 35f87f71c876bd9a827a0e4dd007cafaa8d28c9d9739f91e15187c4ed5c1b891
054 hc6528_400_4_Qu_054_T1270C_t22300s_short.xye 1270 °C 22300 short 1.16 5e67ffeeaa169fc4bb1588c132272a071792fbdc236a0ddb1072af1d73701703
055 hc6528_400_4_Qu_055_T1270C_t22562s_short.xye 1270 °C 22562 short 1.16 1f41d693cd4e4d70be45dfc9b0ac7f7a7332fb6cd104ca9a2eb3ec457a59a984
056 hc6528_400_4_Qu_056_T1270C_t22824s_short.xye 1270 °C 22824 short 1.16 32cf0823e5cb042612255940d25a38be49797e5fc6543ef3e6bf1498d6066749
057 hc6528_400_4_Qu_057_T1270C_t23086s_short.xye 1270 °C 23086 short 1.16 f570ca2061afc8e2e613578df99207b4bc76fcc150d05ed14d65078e652a971a
058 hc6528_400_4_Qu_058_T1270C_t23346s_short.xye 1270 °C 23346 short 1.16 f513f0d6a605d3976ea4d3ff54523d68d5cd4583456c317099020f92a5ff97c6
059 hc6528_400_4_Qu_059_T1270C_t23610s_short.xye 1270 °C 23610 short 1.16 1b42bf976b6efd02b7674de2706b7087e356d61a784cae1c1dd59895234b626a
060 hc6528_400_4_Qu_060_T1270C_t23870s_short.xye 1270 °C 23870 short 1.16 b332f1db7806a6672fb83465eb0f23311cfefb2eb7a2b9ff16a16ae86e9f8c32
061 hc6528_400_4_Qu_061_T1270C_t24132s_short.xye 1270 °C 24132 short 1.16 f2617d330e66752bbd53ed586d9fd98f9e1b3e13b87f02c7587aee6a6a49eebe
062 hc6528_400_4_Qu_062_T1270C_t24394s_short.xye 1270 °C 24394 short 1.16 4c52b39651b676067dfc58eec6aa975a8ee167611dde133e512d61d7c170a009
063 hc6528_400_4_Qu_063_T1270C_t24656s_short.xye 1270 °C 24656 short 1.16 d8bd11f931239651b5e6ec509e640281723c5b2bff8d34f2da391135d30752ba
064 hc6528_400_4_Qu_064_T1270C_t24918s_short.xye 1270 °C 24918 short 1.16 61fa207f2256137c239bdf82e876be508370636ccd9ada1ec070bfb061653865
065 hc6528_400_4_Qu_065_T1270C_t25180s_short.xye 1270 °C 25180 short 1.16 ba950a9f78ea2e1c4022f09d380e0317a071ebc72beb0b09a449cfab937b60e6
066 hc6528_400_4_Qu_066_T1270C_t25442s_short.xye 1270 °C 25442 short 1.16 d8a5f2b4da8133130835a905243ef5b82ab482b3bdbfd1f226aab4ac4c81d4d8
067 hc6528_400_4_Qu_067_T1270C_t25704s_short.xye 1270 °C 25704 short 1.16 fbcbdfc493a9e4244acae2aef4c28076c796afa28bfe1edebf24ca21fcb4bb12
068 hc6528_400_4_Qu_068_T1270C_t25964s_short.xye 1270 °C 25964 short 1.16 97df89646a1e5f1179717577f3fbbffc795b0ff707a63a863dcec92b7b9bf6f0
069 hc6528_400_4_Qu_069_T1270C_t26228s_short.xye 1270 °C 26228 short 1.16 bff295e3a7da2b08a162f6c382a3be58ebceb3e28e2799731d7541c1831f22e4
070 hc6528_400_4_Qu_070_T1270C_t26516s_short.xye 1270 °C 26516 short 1.16 566aefb83da0570a1622365dab01bac74c3b1b323760a9d521d90fad1559eb9a
071 hc6528_400_4_Qu_071_T1272C_t26806s_short.xye 1272 °C 26806 short 1.16 814bd17b5fda244ce7a2aeef81387b981ca3001f26739effa0265f3e741b06b2
072 hc6528_400_4_Qu_072_T1275C_t27066s_short.xye 1275 °C 27066 short 1.16 08dc60ceac38e4890a15fd51f9f747ab40fa96fc09da0ead8841b64142a0e85b
073 hc6528_400_4_Qu_073_T1275C_t27328s_short.xye 1275 °C 27328 short 1.16 388da7e725f23d2e6a2d185d0f725acb263857c3ca0d58be8e3a0caa03cf1378
074 hc6528_400_4_Qu_074_T1275C_t27590s_short.xye 1275 °C 27590 short 1.16 60b1ad3745f73396cb78c4d93ce0fc37c3e271b402a2559901b11c241cca7239
075 hc6528_400_4_Qu_075_T1275C_t27850s_short.xye 1275 °C 27850 short 1.16 85c249b5514be625507ee7c520495d438f52829b361488065af48b6d2a7f3a42
076 hc6528_400_4_Qu_076_T1275C_t28110s_short.xye 1275 °C 28110 short 1.16 7415c5bf34cd7fbcdc260c3fee4bda1ae4d87b920d0f212c5ec01f0ea0b88b54
077 hc6528_400_4_Qu_077_T1275C_t28372s_short.xye 1275 °C 28372 short 1.16 34e16e56c55a4e72ece78efc401c36198f97807faa04da7a25a0deb000b2d259
078 hc6528_400_4_Qu_078_T1275C_t28634s_short.xye 1275 °C 28634 short 1.16 bbe1f434b8b35c1213c9807c84848c25cd1e7a3fe901e30f215ad86765d5c837
079 hc6528_400_4_Qu_079_T1275C_t28904s_short.xye 1275 °C 28904 short 1.16 4a69442a737b91b3617b774f2def8cf434143b3a0b3a07f104d06bf3a4d6fb72
080 hc6528_400_4_Qu_080_T1280C_t29164s_short.xye 1280 °C 29164 short 1.16 de562404f2f513c7709e788686ca594774459e4bfe92391d3c5bea5f844ca71e
081 hc6528_400_4_Qu_081_T1280C_t29426s_short.xye 1280 °C 29426 short 1.16 f97488e29b0c6111f369f4242514785a1b78d66f86cdf7e09a9b0f22bca47205
082 hc6528_400_4_Qu_082_T1280C_t29692s_short.xye 1280 °C 29692 short 1.16 04e0889c7ab6599a16faea28df54ad2a8f2abb90838cfdecff65d87c6bf0ac74
083 hc6528_400_4_Qu_083_T1280C_t29950s_short.xye 1280 °C 29950 short 1.16 204b5996a04e35e0c565793d9bd550f81174ecf8903c03e71a8ae25e9b64bc84
084 hc6528_400_4_Qu_084_T1290C_t30726s_long.xye 1290 °C 30726 long 1.16 9e22163653706b0971287d169fda66da9800432a42d08d8267518130bd4e220e
085 hc6528_400_4_Qu_085_T1290C_t31630s_short.xye 1290 °C 31630 short 1.16 96f4141286688b1cfb6162cfc8ecb7e9bfb5b179c01d0d4a287bd6b2a3252f5e
086 hc6528_400_4_Qu_086_T1299C_t32088s_short.xye 1299 °C 32088 short 1.16 128b191bc935996947d4390cd3dbb7fba35f019622525623b70f5ec189426777
087 hc6528_400_4_Qu_087_T1300C_t32348s_short.xye 1300 °C 32348 short 1.16 4b59f25042180fee5f33a6923252dfd36d69c915cf806bfee8d3526499a6ad44
088 hc6528_400_4_Qu_088_T1300C_t32610s_short.xye 1300 °C 32610 short 1.16 fe3ab3aca797056716b3d23176ed1e83a7e54ff718ed9f4800a9f0787af2b785
089 hc6528_400_4_Qu_089_T1300C_t32872s_short.xye 1300 °C 32872 short 1.16 0088bc588d7f0e8497c30bfa1bdba918a58c78ece249f406132f130cb553c18d
090 hc6528_400_4_Qu_090_T1300C_t33132s_short.xye 1300 °C 33132 short 1.16 8281ee3a04c24cb07b2a47eec6e7174ee84f31b51052bfcc23da3a2002d11d69
091 hc6528_400_4_Qu_091_T1300C_t33394s_short.xye 1300 °C 33394 short 1.16 bdc3de4b5b6eceec0c3fcd9ffe25d6b6a8d890a40f2daee3931a8a6c06cffb66
092 hc6528_400_4_Qu_092_T1300C_t33658s_short.xye 1300 °C 33658 short 1.16 747c5a361dbfbb5f0576f3d09d39eb3b9e64fae34a8364b8a386aff5d2341e33
093 hc6528_400_4_Qu_093_T1300C_t33920s_short.xye 1300 °C 33920 short 1.16 5d81d8954ae5043cf5f926d51e6e13c62c17375edaa69c7de7f6d2da465f8376
094 hc6528_400_4_Qu_094_T1300C_t34182s_short.xye 1300 °C 34182 short 1.16 62c82f99d45a865beb9d8ac8736b5433e0e4faec6b10d660d2bcd28869cd81fe
095 hc6528_400_4_Qu_095_T1300C_t34444s_short.xye 1300 °C 34444 short 1.16 ff4af98e24e8a08abe4ebe77f6122450593bc13ae8010967107765510554b108
096 hc6528_400_4_Qu_096_T1300C_t34704s_short.xye 1300 °C 34704 short 1.16 d5a866876dc8035d2838526ca2d06b6cd73969550100ad7cfb3dba492a47232f
097 hc6528_400_4_Qu_097_T1300C_t34966s_short.xye 1300 °C 34966 short 1.16 b620206fa4cb2952b7b8b59258972e5a36ad79890963983c0490e1bb87b03394
098 hc6528_400_4_Qu_098_T1300C_t35228s_short.xye 1300 °C 35228 short 1.16 8c893f07f97585b4bae29084fffc2534f7b543816ceeb9bfd7071b9101cf45dc
099 hc6528_400_4_Qu_099_T1300C_t35490s_short.xye 1300 °C 35490 short 1.16 aab222d6856bf2d1c6955eef21c2f38d5b57949abc9e5bcdaf7f70637304438a
100 hc6528_400_4_Qu_100_T1300C_t36128s_long.xye 1300 °C 36128 long 1.16 156508520b93412c6925350d4b6ee8cbc55ab3c032bf206197e0c814da670adf
101 hc6528_400_4_Qu_101_background_nosample_t38192s_long.xye background, no sample 38192 long 1.16 58674923c560e4b6678ff0aa11cbd80ca5e61eb741c19af7869dea50bcee0926

How to use them

  • The format. Plain text, three columns per line: 2θ in degrees (0.001° step to 26.999°), intensity in counts after the beamline's normalisation, estimated standard deviation. No header. The first 0.02° is the beamstop's shadow (zero intensity, large esd). See Data: file format.
  • The names. hc6528_400_4_Qu_<seq>_T<temp>C_t<elapsed>s_<long|short>.xye: sequence, nominal temperature, seconds since the first scan, exposure class. The scheme and the original names: Data: naming.
  • In any program. Every powder-diffraction program reads three-column .xye (Topas, GSAS-II, FullProf through its XY formats, Python with numpy.loadtxt).
  • In diff-ref-struct. Unpack the scans into a folder Data/ and the sets zip beside it; drs plots open Plots/hold-1270.drv reads a set, drs-publish build Publish/esrf-series.drp remakes the projections, the app's Plots module opens any .drv with its Projection, Map and Surface views. The maps need the scans rebinned by the core; the README in the zip gives the two commands.
  • Check what you got. The SHA-256 of every file is in the index and in the table; shasum -a 256 <file> on a Mac, sha256sum on Linux.